Molecular Distillation is a special liquid-liquid separation technology, which is carried out under high vacuum environment. It uses the differences in the free path of molecular motion of different substances to achieve separation.
DOVMXtech is China's best quality Molecular Distillation / Thin Film Evaporator equipment supplier.
There are three types of DOVMXtech series molecular distillation:Glass Molecular Distillation Unit, Hybrid Molecular Distillation Unit, Stainless Steel Molecular Distillation Unit. These are mainly applicable to the pilot production scale, especially the separation and extraction of high-quality hemp oil CBD / THC, fish oil EPA / DHA and plant essential oil.
Our short path molecular distillation system is very suitable for distillation/purification of heat sensitive material or high boiling point material. Short path distillation is widely used in chemical, pharmaceutical, petrochemical, spices, plastics, oil and other fields.
The lactic acid prepared by fermentation method can yield L2 lactic acid, D2 lactic acid, and DL2 lactic acid depending on the selected strain and fermentation conditions. These are crude lactic acids with low purity. With the increasing demand for high purity L2 lactic acid, it is of great significance to purify and refine L2 lactic acid.
When using ordinary vacuum distillation to separate and purify lactic acid, it is difficult to reach a lower pressure in the system, resulting in poor heat resistance and easy decomposition of the evaporated lactic acid. The molecular distillation method can be operated at a far lower pressure than normal pressure, resulting in high purity of lactic acid and good heat resistance. Therefore, the molecular distillation method is significantly superior to ordinary vacuum distillation operated under boiling state.
DOVMX is the first brand of wiped film molecular distillation in China, with excellent quality, stable operation, and reasonable price. We have previously customized stainless steel reactors and molecular distillation equipment for lactic acid extraction and purification for our customers. Our equipment is specifically optimized for the extraction and purification of lactic acid. Low purity lactic acid does not require other dehydration and decolorization processes, but only requires the molecular distillation method under our guidance to obtain high purity L2 lactic acid. At the same time, after using our complete set of equipment, we will provide technical assistance and guidance, including the adjustment of rotational speed, temperature, vacuum degree, and operating methods, to obtain L2 lactic acid with a purity of more than 95%.
DOVMXtech molecular distillation:
Selling point
- Years of design and production experience, a large number of installation cases, high quality and reasonable price;
- The equipment is scientific in design, safe and reliable, stable in operation, simple in operation, and fast in turnkey installation;
- The equipment can pass the US UL certification and European CE certification;
- DOVMXtech brand is well-known worldwide;
- We are a well-known OEM supplier of laboratory equipment in the United States and Canada;
- Equipment can be customized according to customer requirements;
- We can provide door-to-door transportation services, worry-free delivery, including customs clearance;
- Recruit distributor partners worldwide. We have a very mature dealer pricing system that fully guarantees the interests of dealers.
(DOVMXtech molecular distillation) | ||||||
Model | FMD-60 | FMD-80 | FMD-100 | FMD-150 | FMD-200 | FMD-230 |
Evaporation area (M2) | 0.06 | 0.1 | 0.15 | 0.25 | 0.35 | 0.5 |
Reference handling capacity(L/H) | 0.5-1.0 | 1.0-5.0 | 2.0-10 | 3.0-15 | 4.0-20 | 6.0-30 |
Feed tank volume(L) | >2.0 | >2.0 | 3 | >3.0 | >5.0 | >10.0 |
Feeding method | Manual knob valve feed (default) | |||||
Peistaltic pump feed (optional) | ||||||
Gear pump, automatic continuous feeding, adjustable speed (optional) | ||||||
Discharge method | Discharge after shutdown (default) | |||||
Manual discharge (optional) | ||||||
Gear pump, automatic continuous discharging , adjustable speed (optional) | ||||||
Vacuum (mbar) | (Reachable) 0.001 mbar | |||||
Speed range (rpm) | 0-450 | 0-300 | ||||
Operating temperature | (The highest temperature can reach) 300°C | |||||
Insulation method | Heating with electric heating tape | |||||
Double jacket, heated with heat transfer medium |
Type C has the same parameters as type A. Type C is the jacketed version of type A.
Model DOVMXtech |
Effective evaporation area (M2) | Condensation area (M2) | Barrel Inside diameter (mm) | Feeding funnel volume (L) | Processing flow (KG/H) | Power (W) | Max rotation speed (RPM) |
MD-60A | 0.05 | 0.1 | 60 | 1.5 | 0.1-2.0 | 120 | 450 |
MD-80A | 0.1 | 0.15 | 80 | 1.5 | 0.3-4.0 | 120 | 450 |
MD-100A | 0.15 | 0.2 | 100 | 1.5 | 0.5-5.0 | 120 | 450 |
MD-150A | 0.25 | 0.4 | 150 | 1.5 | 1.0-8.0 | 120 | 450 |
MD-200A | 0.35 | 0.5 | 190 | 1.5 | 1.5-10.0 | 200 | 300 |
MD-230A | 0.5 | 0.65 | 220 | 1.5 | 2.0-15.0 | 200 | 300 |
1, High evaporation efficiency and reduced retention time, with minimal time delay.
2, Short path distillation is made from high borosilicate glass 3.3, stainless steel 316L and PTFE, which has excellent corrosion resistance.
3, Main body of Short path distillation is made of high borosilicate glass 3.3, allowing the whole process to be observed very clearly.
4, High precision PTFE rollers and inner glass surface allow the liquid to form a complete and unified thin film on the heated surface. The smooth inner surface, avoid stick and scaling.
5, Magnetic force transmission makes film forming system separate from motor. The whole System performs a completed sealing. The minimum vacuum pressure is down to 0.001mbar.
6, Highest temperature of the system can reach 230℃/300℃, accurate temperature control can be realized.
7, Scraper Model and self-cleaning roller Model film forming system are available.
8, For the material of distiller barrel, both glass and stainless steel available.
9, Heavy-duty stainless steel frame with swivel casters and leveling feet for mobility and stability.
10, Turnkey package which is plug-and-play, technical supports available.
11, The latest version Cold Trap, we customized the ultra-low temperature probe cooler down to -100°C(no dry ice needed)(optional)
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Short Path Molecular Distillation DOVMXtech FMD-A descripttion:
DOVMX FMD series Wiped Film Molecular Distillation Equipment Model FMD-60A FMD-80A FMD-100A Main Evaporator Jacketed Glass Barrel with Internal Cooling Condenser
Borosilicate Glass 3.3
Glass jacket volume: approx. 3L-5LHeated circulator: 3kW heater, 0°C-300°C maximum operating temperature Evaporation area(m2) 0.06 0.1 0.15 Internal diameter of main evaporator (inch) 2 3 4 Condensation area (M2) 0.1 0.15 0.2 Main Condenser Material: borosilicate glass 3.3
Style: coil
Glass jacket volume: approx. 1.5L-2.2LCooling/heated circulator: 2kW heater, -25°C to 200°C operating temperature Process rate(L/H) 0.5-2 1-3 1-4 base on processes and material fed Feeding tank(L) 5L 5L 5L glass, jacketed, with lid, refillable manually during operation.
Number of Ports on the Lid: Three
Port Size: 24/40vacuumized with a vacuum pump(Optional, not standard) Heated circulator(Optional, not standard, recommended):
2kW heater, 200°C maximum operating temperature
Recommended circulating thermal fluid temperature: 80°C to 120°CFeeding method 1.Manual regulating valve natural flow feeding 2.Gear pump / peristaltic pump(Optional, not standard, recommended):
Gear pump for automatic and continuous feeding, speed adjustable
Speed: 20L/hour max. (2.4 mL/turn, 135 turn/minute), adjustable
Material: stainless steel body with Viton gaskets
Peristaltic pump module with connections, for continuous inlet
Pump rate: 1-720ml/min
Speed rate: 0.1-150RPM
Power: 40W
Electricity: 100-240VFeeding System heated stainless steel tubing by winding electric heating belt Wiping scattering system Style: roller and blade
Driving motor: the connection of the scatterer magnetic coupling
Roller/blade material:
316L stainless steel scatterer roller with PTFE blades
Motor power: 200 W
Speed of scatterer adjustable:0-450 rpm 0-450 rpm 0-450 rpm Receiving part Distillate Discharge:
Receiving flask x 2
volume: 10L, glass, Drain valve, Port: Spherical Joint
Drain passage: non-heated
Sealing gasket: VitonResidue Discharge:
Receiving flask x 2
volume: 10L, glass, Drain valve, Port: Spherical Joint
Drain passage: heated by winding electric heating tape
Sealing gasket: Viton
Recommended circulating thermal fluid temperature: 80°C to 120°CReceiving Discharging method continuous collection discharge
Connections with Glass/PTFE Vacuum block valve(upgraded)
Receiving flask with Manual regulating Drain valve(upgraded)Vacuum level(mbar) Vacuum pump, Low to 0.001mbar vacuum pump with a diffusion pump(Optional, not standard)
Diffusion Pump
Diameter: 100mm
End vacuum : 5*10-2pa
Pump rate: 80L/S
Heating Power: 500W
Electricity: 220VCold Trap cooler Material: borosilicate glass with polyethylene lid
Depth: 17"
Receiving flask x 2
volume: 2LCooling mode: Dry ice Cooling mode: Immersion cooler(Optional, not standard, recommended):
Low Temperature Cooler, 3" Rigid Stainless Steel Coil Probe for cold trap
Ultra-low temperature cooler (air-cooled)
Minimum temperature - 100°C
Temperature control range: - 100°C~- 60°C (customers need to control the temperature at - 80°C)Heated circulator
(Heating thermostat I)
for Feeding tanktemperature range: 45 to 200°C,
minimum heating power: 2.0 kW
stainless steel bath
bath capacity: 5L-10 L
power supply: 230 V, 50 Hz
TFT color touch screen display not less than 5.7”
setting and current reading of the process temperature with a resolution of 0.1°C,
real-time clock
internal liquid pressure control system,
regulation of heating power,
setting of temperature limits
visual and audible alarms,
alarm for exceeding safety temperature and liquid level
automatic restart of the system after power interruption
pump speed control mode
system degassing function,
maximum pump pressure no worse than 27 /min / 0.7 bar,
maximum suction power not worse than 22 L/min / 0.4 bar;Heated circulator
(Heating thermostat II)
for Main EvaporatorTemperature range: from 30 to 300°C,
minimum heating power: 5 kW
stainless steel bath,
bath capacity: 30 L,
power supply: 230 V, 50 Hz,
TFT color touchscreen display not less than 5.7”
setting and current reading of the process temperature with a resolution of 0.1°C,
real-time clock
internal liquid pressure control system
regulation of heating power
setting of temperature limits
alarm for exceeding safety temperature and liquid level
pump speed control mode,
system degassing function,-
maximum pump pressure no worse than 25 L/min / 0.7 bar,
maximum suction power not worse than 18.5 L/min / 0.4 barCooling/heated circulator
(heating-cooling circulator I)
for Main Condenser columnOperating range: -25 to 100°C ,
Minimum cooling power:
at 0°C: 1 kW,
at -10°C: 0.7 kW,
at -20°C: 0.25 kW,
Pump capacity: from 20 to 28 L/min,
Filling capacity of 3.8 L,
Minimum filling capacity of not more than 1.7 L,
Dimensions not more than 420x490x580 mm,
Power supply: 230 V, 50 Hz;vacuum pump 8 L/S or 28.8 m3/h
oil-based, two-stage,
motor power: min. 850 W,
minimum final vacuum: at least 3*10-3 bar,
outlet filter;Electrical Control Cabinet Digital display,
Pirani Vacuum Gauge with LCD display for high vacuum application(0.01pa-1atm)
Wiper motor controller x 1
Gear pump controller x 1(Optional, not standard)
Two Temperature Controllers for Heating Tapes
(Feeding tubing heater controller x 1
Residue discharge heater controller x 1)
Main power switch x 1
Vacuum pump switch x 1
Diffusion pump switch x 1(Optional, not standard)
230V +/-5V, 1~phase 60Hz (50Hz power for Europe and Asia available upon request)Main Mounting Frame constructed of Heavy-duty stainless steel (304),
mounted on four swivel casters with leveling feet,
stable structure to ensure the mobility of the device (swivel wheels with lock)Dimensions L*W*H(cm) 240*70*210 250*80*260 260*90*280 Other accessories A set of connecting cables for the heating, cooling and vacuum system;
Cork mat x 2;
Stainless steel lifting table x 2;
seal ring x 12;
Vacuum Tubes;
Imported silicone hose;
Heating/Chilling Hoses;
Heating belt/Heating tape x 2;
fixture;
Several other accessories;
(Oil and liquid need to be purchased and transported separately)
Silicone oil
viscosity at 25°C: 20 mm²/s,
capacity min. 25 L,
Thermostat oil with technical parameters
open systems range: -20°C-195°C,
closed systems -20°C-235°C,
Oil for chillers with technical parameters
temperature range from -20°C to 40°C,
viscosity at 25°C: mm²/s,
capacity of 20 L
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DOVMXtech-FMD-60A
Throughput
0.3 to 1.0L per hour **
Main Evaporator
Evaporating area: approximately 350 cm²
Glass jacket volume: approx. 0.5L
Heated circulator: 3kw heater, 300 °C maximum operating temperature
Main Condenser
Condensing area: approximately 550 cm²
Glass jacket volume: approx. 0.35L
Cooling/Heated circulator: 2kw heater, -25 °C to 200 °C operating temperature
Wiping System
Style: PTFE Roller
Driving motor: speed-adjustable with magnetic coupling
Cold Trap
Material: borosilicate glass with polyethylene lid
Receiving flask volume: 500ml
Feeding System
Glass Flask volume: 1L, jacketed, refillable during operation
Flask jacket volume: approx. 0.5L
Heated circulator: 3kw heater, 300 °C maximum operating temperature
Distillate Discharge Receiving flask volume: 500ml, glass
Residue Discharge Receiving flask volume: 500ml, glass
Vacuum System
Vacuum gauge: included
Vacuum pump: flow rate 4L/S
Sealing gasket All food grade Viton
Mounting Frame Heavy duty stainless steel, mounted with 4 rubber feet
Main Power
230V, 60Hz, 1 Phase
Unit dimensions
Approx. 61"W x 22"D x 53"H
Unit weight
Approx. 360 Lbs
Compliance
CE, CSA, UL (upon request)
*Specifications and supporting equipment may change or upgrade at any time.
** Process feed rate may differ based on amount of low boiling molecules in feedstock and SOP.
Optional Supporting Equipment for CSA/UL compliance
SUPPORTING EQUIPMENT Optional
Vacuum Pump
Ultimate Pressure: 3 x 10-3 mbar
Vacuum gauge: included
Heat Circulator
Temperature Range: RT~200°C
Heating Capacity: 2kw
Bath Volume: 6L
Cooling/Heated Circulator
Temperature Range: -20°C~100°C
Cooling Capacity: various
Bath Volume: 6L
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Each equipment will undergo many strict inspections before delivery and transportation to ensure that it is intact. All electrical parts are warranted for one year (except for vacuum pumps and glassware). We have provided double copies for easily damaged items. Please rest assured that the whole machine will be maintained for life. if something breaks, replacement parts will be shipped next day by air.
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